Superparamagnetic bimetallic iron-palladium nanoalloy: synthesis and characterization |
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Authors: | Nazir Rabia Mazhar Muhammad Akhtar M Javed Raza Shah M Khan Nawazish A Nadeem M Siddique Muhammad Mehmood Mazhar Butt N M |
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Affiliation: | Department of Chemistry, Quaid-i-Azam University, Islamabad 45320, Pakistan. |
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Abstract: | Iron-palladium nanoalloy in the particle size range of 15-30?nm is synthesized by the relatively low temperature thermal decomposition of coprecipitated [Fe(Bipy)(3)]Cl(2) and [Pd(Bipy)(3)]Cl(2) in an inert ambient of dry argon gas. The silvery black Fe-Pd alloy nanoparticles are air-stable and have been characterized by EDX-RF, XRD, AFM, TEM, magnetometry, (57)Fe M?ssbauer and impedance spectroscopy. This Fe-Pd nanoalloy is in single phase and contains iron sites having up to 11 nearest-neighboring atoms. It is superparamagnetic in nature with high magnetic susceptibility, low coercivity and hyperfine field. |
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