| 二氧化硅表面负载纳米级SnO_2-CuO复合材料的制备工艺研究 |
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| 引用本文： | 周元臻,杨清翠,徐一峰,何志仙,张思敬,刘静.二氧化硅表面负载纳米级SnO_2-CuO复合材料的制备工艺研究[J].应用化工,2011,40(3):428-430. |
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| 作者姓名： | 周元臻 杨清翠 徐一峰 何志仙 张思敬 刘静 |
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| 作者单位： | 西安建筑科技大学理学院,陕西,西安,710055 |
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| 基金项目： | 陕西省自然科学基础研究基金项目，陕西省教育厅专项科研项目 |
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| 摘 要： | 以有机改性的SBA-15为载体,采用化学共沉积法制备了一种负载纳米金属氧化物SnO2-CuO/SBA-15新型材料,通过IR、UV和SEM表征其结构和形貌。考察了影响材料性能的几个主要参数。通过正交实验得到工艺优化条件为:原料配比n(Sn)∶n(Cu)=1∶3,反应时间为3 h,反应温度为70℃。
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| 关 键 词： | SBA-15 共沉积法 SnO2-CuO |
Technological research of mesoporous composite material loaded nanometer SnO2-CuO |
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| ZHOU Yuan-zhen,YANG Qing-cui,XU Yi-feng,HE Zhi-xian,ZHANG Si-jing,LIU Jing.Technological research of mesoporous composite material loaded nanometer SnO2-CuO[J].Applied chemical industry,2011,40(3):428-430. |
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| Authors: | ZHOU Yuan-zhen YANG Qing-cui XU Yi-feng HE Zhi-xian ZHANG Si-jing LIU Jing |
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| Affiliation: | ZHOU Yuan-zhen,YANG Qing-cui,XU Yi-feng,HE Zhi-xian,ZHANG Si-jing,LIU Jing(School of Science,Xi'an University of Architecture and Technology,Xi'an 710055,China) |
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| Abstract: | A novel composite material of mesoporous SBA-15 loaded nanometer SnO2-CuO was prepared by grafting and chemical coprecipitation.Characteristics of mesoporous composite material were investigated by IR,UV and SEM.The orthogonal experiment results show that the optimum technological conditions were as follows:n(Sn)∶ n(Cu) were 1∶ 3,reaction time and reaction temperature were 3 h and 70 ℃,respectively. |
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| Keywords: | SBA-15 SnO2-CuO |
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