| 环酰菌胺的合成 |
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| 引用本文： | 凌岗,刘晓智.环酰菌胺的合成[J].农药,2009,48(5). |
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| 作者姓名： | 凌岗 刘晓智 |
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| 作者单位： | 1. 江苏盐城工学院,化学与生物工程学院,江苏,盐城,224051
2. 辽宁大学,稀散元素研究所,沈阳,110036 |
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| 摘 要： | 以(2,3-二氯-4-羟基苯基)偶氮苯为原料,制备了2,3-二氯-4-羟基苯胺,收率为90%;然后与1-甲基环己基甲酰氯反应制备标题化合物环酰菌胺,此步反应收率达92.4%.两步反应总收率为83.2%.
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| 关 键 词： | 环酰菌胺 杀菌剂 灰霉病 合成 |
Synthesis of Fenhexamid |
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| LING Gang,LIU Xiao-zhi.Synthesis of Fenhexamid[J].Pesticides,2009,48(5). |
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| Authors: | LING Gang LIU Xiao-zhi |
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| Affiliation: | 1.Jangsu Yancheng Institute of Technology;Chemical&Biological Engineering School;Yancheng 224051;Jiangsu;China;2.Institute of Rare and Scattered Metals Chemistry;Liaoning University;Shenyang 110036;China |
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| Abstract: | The fungicide of fenhexamid was synthesized by reacting 1-methylcylohexanecarboxylic acid chloride with 4-hydroxy-2,3-dichloroaniline prepared by reducing of(2,3-dichloro-4-hydroxyphenyl)phenyldiazene(the yield was 90%).The fenhexamid yield was 92.4%and the whole yield of the two reactions was 83.2%. |
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| Keywords: | fenhexamid fungicide grey mold synthesis |
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