| 氮杂杯[6]芳烃迭氮化衍生物的合成与表征 |
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| 引用本文： | 王晶,曹端林,胡志勇,张文艳.氮杂杯[6]芳烃迭氮化衍生物的合成与表征[J].应用化工,2009,28(1). |
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| 作者姓名： | 王晶 曹端林 胡志勇 张文艳 |
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| 作者单位： | 中北大学,化工与环境学院,山西,太原,030051 |
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| 摘 要： | 以氮杂杯6]芳烃和迭氮化钠为原料,四氢呋喃为溶剂,在为40~45℃合成了氮杂杯6]芳烃迭氮化衍生物,通过薄层色谱分析法、红外光谱分析法和核磁共振氢谱法对产物进行了表征,证实其为目标产物,从而验证了合成路线的可行性。
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| 关 键 词： | 氮杂杯[6]芳烃 迭氮化衍生物 表征 |
Synthesis and characterization of aza-bridged calix[6]arene azides-derivative |
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| WANG Jing,CAO Duan-lin,HU Zhi-yong,ZHANG Wen-yan.Synthesis and characterization of aza-bridged calix[6]arene azides-derivative[J].Applied chemical industry,2009,28(1). |
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| Authors: | WANG Jing CAO Duan-lin HU Zhi-yong ZHANG Wen-yan |
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| Abstract: | In this paper,ultimate production aza-bridged calix6]arene azides-derivative was synthesized from aza-bridged calix6]arene and sodium azide in the experiment,THF as solvent,at 40～45 ℃.The product is characterized through TLC,FT-IR and 1H NMR.It is proved that it is the target product,consequently synthesis path is feasible. |
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| Keywords: | aza-bridged calix[6]arene azides-derivative characterize |
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