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Evaluating Pore Space in Macroporous Ceramics with Water‐Based Porosimetry
Authors:Linnéa Andersson  Per Tomas Larsson  Lars Wågberg  Lennart Bergström
Affiliation:1. Department of Materials and Environmental Chemistry, Stockholm University, , SE‐106 91 Stockholm, Sweden;2. WWSC, Wallenberg Wood Science Center, , SE‐100 44 Stockholm, Sweden;3. Innventia AB, , SE‐114 86 Stockholm, Sweden;4. Department of Fibre and Polymer Technology, School of Chemical Science and Engineering, Royal Institute of Technology, , SE‐100 44 Stockholm, Sweden
Abstract:We show that water‐based porosimetry (WBP), a facile, simple, and nondestructive porosimetry technique, accurately evaluates both the pore size distribution and throat size distribution of sacrificially templated macroporous alumina. The pore size distribution and throat size distribution derived from the WBP evaluation in uptake (imbibition) and release (drainage) mode, respectively, were corroborated by mercury porosimetry and X‐ray micro‐computed tomography (μ‐CT). In contrast with mercury porosimetry, the WBP also provided information on the presence of “dead‐end pores” in the macroporous alumina.
Keywords:
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