| 共沉淀法制备纳米氧化镁的研究 |
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| 引用本文： | 张浦,侯建国,张芳.共沉淀法制备纳米氧化镁的研究[J].河南化工,2007,24(6):24-25,40. |
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| 作者姓名： | 张浦 侯建国 张芳 |
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| 作者单位： | 南昌理工学院,生物与环境工程系,江西,南昌,330013 |
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| 摘 要： | 以氯化镁与碳酸钠为原料,采用共沉淀法,研究了反应溶液的pH值、反应物浓度、反应温度、反应时间和煅烧温度对制备纳米氧化镁粉体的影响,通过透射电镜(TEM)、X射线衍射(XRD)、热重分析(TG)对样品的性能进行测试,获得纳米氧化镁平均粒径约12 nm,且分布较均匀.
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| 关 键 词： | 纳米 氧化镁 制备 共沉淀法 共沉淀法 法制 纳米氧化镁 研究 Method Sedimentation Nanometer Preparation 均匀 分布 平均粒径 测试 性能 样品 热重分析 射线衍射 透射电镜 影响 氧化镁粉体 煅烧温度 |
| 文章编号： | 1003-3467（2007）06-0024-02 |
| 修稿时间： | 2007-03-26 |
Research on Preparation of Nanometer MgO with the Sedimentation Method |
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| ZHANG Pu,HOU Jian-guo,ZHANG Fang.Research on Preparation of Nanometer MgO with the Sedimentation Method[J].Henan Chemical Industry,2007,24(6):24-25,40. |
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| Authors: | ZHANG Pu HOU Jian-guo ZHANG Fang |
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| Affiliation: | Department of Biology and Environment Engineering , Nanchang Institute of Technology , Nanchang 330013 , China |
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| Abstract: | The nanometer MgO is prepared by the sedimentation method with MgCl2 and Na2CO3 as raw materials.The main influencing factors,such as pH value of the reaction,the reactant density,the reaction temperature,and the calcining temperature for preparing nanometer MgO powder are investigated.The property of MgO sample is tested with the transmission electronic microscope(TEM),the X-ray diffraction analysis(XRD) and the thermogravimetry(TG). The product has an average diameter of 12 nm with good sphere-shaped. |
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| Keywords: | nanometer MgO preparation sedimentation method |
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