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钛白副产硫酸亚铁制备超细透明氧化铁黄研究
引用本文:李金磊,胡兵,宋建民. 钛白副产硫酸亚铁制备超细透明氧化铁黄研究[J]. 湖北工业大学学报, 2012, 27(2): 64-66
作者姓名:李金磊  胡兵  宋建民
作者单位:湖北工业大学化学与环境工程学院,湖北武汉,430068
摘    要:以钛白粉厂副产物硫酸亚铁为原料,以氨水为沉淀剂,采用空气氧化法制备超细透明氧化铁黄.分别研究了影响晶种形成和晶体生长的主要影响因素.通过优化实验,得出了最佳工艺条件.晶种制备阶段:温度为30℃,空气流量为2L/min,溶液的pH为4~6,搅拌速度为400r/min,Fe2+浓度为1mol/L.晶体生长阶段:温度为85℃,空气流量为2L/min,溶液pH为4~6.

关 键 词:钛白粉  硫酸亚铁  氧化铁黄  空气氧化法

Preparation of Superfine Transparent Iron Oxide with Ferrous Sulphate from the By-product of Titanium Dioxide Production
LI Jin-lei,HU Bing,SONG Jian-min. Preparation of Superfine Transparent Iron Oxide with Ferrous Sulphate from the By-product of Titanium Dioxide Production[J]. Journal of Hubei University of Technology, 2012, 27(2): 64-66
Authors:LI Jin-lei  HU Bing  SONG Jian-min
Affiliation:(School of Chemical & Environmental Engin.,Hubei Univ.of Tech.,Wuhan 430068,China)
Abstract:A process of preparing superfine transparent iron oxide with the by-products of ferrous sulfate was described.The process included two steps:the yielding and growing of crystals.Several key factors affecting the two steps were studied respectively such as effects of Fe2+ concentration,air flow rate and stirring rate and reaction temperature and pH values.
Keywords:ferrous sulphate  air oxidation  iron oxide yellow pigment  preparation
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