| 二水合5,5'-联四唑-1,1'-二羟基的纯度分析方法 |
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| 引用本文： | 熊书玲,陈树森,李丽洁,金韶华,束庆海,童宗睿,李京霖. 二水合5,5'-联四唑-1,1'-二羟基的纯度分析方法[J]. 含能材料, 2016, 24(2): 209-212. DOI: 10.11943/j.issn.1006-9941.2016.02.017 |
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| 作者姓名： | 熊书玲 陈树森 李丽洁 金韶华 束庆海 童宗睿 李京霖 |
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| 作者单位： | 1. 北京理工大学材料学院,北京,100081;2. 甘肃银光化学工业集团公司,甘肃白银,730900 |
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| 基金项目： | 青年科技创新项目(3090041310045) |
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| 摘 要： | 建立了二水合5,5'-联四唑-1,1'-二羟基(BTO)纯度的高效液相色谱分析条件:反相色谱柱(Sino Chrom ODS-BP,4.6 mm×200 mm,5μm),检测波长213 nm,二元流动相乙腈-水30/70(V/V),流速1.0 m L·min-1,柱温25℃。采用外标法对BTO标准溶液进行定量测定,BTO浓度(c)在0.12~0.60 mg·m L-1范围内与色谱峰峰高(h)呈良好的线性关系,线性方程为h=573.78c-1.18,线性相关系数为0.9998。该法的相对标准偏差为0.48%~1.00%,平均回收率为98.10%~100.64%,方法灵敏、准确,可用于BTO产品的纯度分析。
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| 关 键 词： | 高效液相色谱 纯度分析 外标法 二水合5,5'-联四唑-1,1'-二羟基(BTO) |
| 收稿时间： | 2015-04-02 |
| 修稿时间： | 2015-05-25 |
Purity Analysis Method of 5,5'-Bistetrazole-1,1 '-dyhydroxy Dihydrate |
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| XIONG Shu-ling,CHEN Shu-sen,LI Li-jie,JIN Shao-hu,SHU Qing-hai,TONG Zong-rui and LI Jing-lin. Purity Analysis Method of 5,5'-Bistetrazole-1,1 '-dyhydroxy Dihydrate[J]. Chinese Journal of Energetic Materials, 2016, 24(2): 209-212. DOI: 10.11943/j.issn.1006-9941.2016.02.017 |
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| Authors: | XIONG Shu-ling CHEN Shu-sen LI Li-jie JIN Shao-hu SHU Qing-hai TONG Zong-rui LI Jing-lin |
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| Affiliation: | School of Material Science and Engineering, Beijing Institute of Technology, Beijing 100081, China,School of Material Science and Engineering, Beijing Institute of Technology, Beijing 100081, China,School of Material Science and Engineering, Beijing Institute of Technology, Beijing 100081, China,School of Material Science and Engineering, Beijing Institute of Technology, Beijing 100081, China,School of Material Science and Engineering, Beijing Institute of Technology, Beijing 100081, China,School of Material Science and Engineering, Beijing Institute of Technology, Beijing 100081, China and Gansu Yinguang Chemical Industry Group Co., Ltd., Baiyin 730900, China |
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| Abstract: | |
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| Keywords: | high performance liquid chromatography (HPLC) purity analysis external standard method 5,5'-bistetrazole-1,1'-dyhydroxy dihydrate(BTO) |
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