| 间接电氧化法合成邻氯苯甲醛 |
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| 引用本文： | 谭和宋. 间接电氧化法合成邻氯苯甲醛[J]. 化工时刊, 1999, 13(3): 17-20,9 |
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| 作者姓名： | 谭和宋 |
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| 作者单位： | 株州化工集团有限责任公司 412004 |
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| 摘 要： | 探索了ＭｎＳＯ４的电解条件，使Ｍｎ＾３＋浓度达到（０．３－０．５）ｍｏｌ／Ｌ，优化了Ｍｎ＾３＋的氧化条件；解决了回收ＭｎＳＯ４的电解问题；实验认为，氧化过程醛的浓度应控制在４％以下讨论了化学法提纯邻氯苯甲醛的可行性。
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| 关 键 词： | 邻氯苯甲醛 间接电氧化 邻氯甲苯 合成 |
Indirect Electrolytic Oxidation Synthetic Process for hte Production of O- chlorobenzaldehyde |
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| Tan Hesong. Indirect Electrolytic Oxidation Synthetic Process for hte Production of O- chlorobenzaldehyde[J]. Chemical Industry Times, 1999, 13(3): 17-20,9 |
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| Authors: | Tan Hesong |
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| Affiliation: | Zhuzhou Chemical Industry Group Lit. Co. |
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| Abstract: | Explored the electrolysis conditions of mangenese sulfate. Made the concentration of Mn3+arriving to (0.3-0.5)mol/L. Made the oxidation condition better. Settled the electrolytic problem of retrieving mangenese sulfate. The conclusion of the experiment is that the concentration of o - chlorobenzaldehyde in the oxidation process should be controled inferior to four percent. Discussed the feasibikity of chemical purifying of o-chlorobenzaldehyde. |
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| Keywords: | o - chlorobenzaldehyde indirect electrolytic oxidation mangenese sulfate o- chlorotoluene. |
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