2—十二烷基二硫代苯并噻唑的合成 |
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引用本文: | 张俊彦 刘维民. 2—十二烷基二硫代苯并噻唑的合成[J]. 化学试剂, 1999, 21(5): 299-300 |
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作者姓名: | 张俊彦 刘维民 |
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作者单位: | 中国科学院兰州化学物理研究所固体润滑开放实验室!兰州730000 |
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摘 要: | 由2-巯基苯并噻唑和十二烷基硫醇在过氧化氢的氧化下合了2-十烷基二硫代苯并噻唑,经元素分析、红外、核磁共振确定为纯品。
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关 键 词: | 润滑油添加剂 合成 十二烷基 二硫代 苯并噻唑 |
The synthesis of 2 ( n dodecyldithio) benzothiazole |
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Abstract: | The synthesis of 2 ( n dodecyldithio) benzothiazole is described.The compound was confirmed by elemental analysis,IR and 1HNMR spectrophotometric techniques. The authors tried to improve its solubility in mineral oil with the introduction of a long chain dodecylgroup,and to assemble an S arrangement with a different bonding structure by introducing a disulphide arrangement besides the heterocyclic sulphur. |
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Keywords: | thiobenzothiazole hydrogen peroxide synthesis |
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