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Solubility of a Russia vacuum residue and group composition of the soluble fractions in different solvents
Authors:Li Han  Zhi-Min Zong  Zheng Wang
Affiliation:1. School of Chemical Engineering and Energy, Zhengzhou University, Zhengzhou, Henan, China;2. Key Laboratory of Coal Processing and Efficient Utilization (Ministry of Education), China University of Mining &3. Technology, Xuzhou, Jiangsu, China;4. lihan@zzu.edu.cn;6. Key Laboratory of Coal Processing and Efficient Utilization (Ministry of Education), China University of Mining &7. Key Laboratory of Energy Resources and Chemical Engineering, Institute of Chemistry and Chemical Engineering, Ningxia University, Yinchuan Shi, Ningxia Huizuzizhiqu, China
Abstract:Abstract

A Russia vacuum residue (RVR) was ultrasonically extracted with 15 organic solvents, respectively. The soluble fractions (SFs) were analyzed with a gas chromatography/mass spectrometer (GC/MS). The results show that the extract yields of RVR largely increased with the decrease in the dielectric constant of solvents, i.e., RVR tends to dissolve in weakly polar and non-polar solvents. Most of GC/MS-detectable components in the SFs are chain alkanes and cyclanes.
Keywords:GC/MS analysis  group composition  solubility  solvent extraction  vacuum residue
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