| 相转移催化合成2-(2,4-二氯苯氧基)三乙胺 |
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| 引用本文： | 何建玲. 相转移催化合成2-(2,4-二氯苯氧基)三乙胺[J]. 化学世界, 2004, 45(11): 586-587,599 |
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| 作者姓名： | 何建玲 |
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| 作者单位： | 盐城工学院化工系,江苏,盐城,224003 |
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| 摘 要： | 以2,4-二氯苯酚为原料,利用相转移催化剂来制备2-(2,4二氯苯氧基)三乙胺。并以正交实验研究和讨论了反应温度、反应时间、反应物摩尔配比、溶液的酸碱性对醚化实验结果的影响,得到最佳反应条件。对所制备的产物进行表征。通过红外光谱、核磁共振氢谱和元素分析确定了目标化合物的结构。
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| 关 键 词： | 2 4-二氯苯酚 相转移催化 正交实验 2-(2,4-二氯苯氧基)三乙胺 |
| 文章编号： | 0367-6358(2004)11-0586-03 |
Synthesis of 2- (2,4-Dichlorophenoxy)triethylamine on Phase-transfer Catalyst |
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| HE Jian-ling. Synthesis of 2- (2,4-Dichlorophenoxy)triethylamine on Phase-transfer Catalyst[J]. Chemical World, 2004, 45(11): 586-587,599 |
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| Authors: | HE Jian-ling |
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| Abstract: | 2-(2,4-Dichlorophenoxy)triethylamine was prepared on phase-transfer catalyst, using 2,4-dichlorophenol as raw material. Based on orthogonal experimental design, the influential factors such as temperature, time and the acid-base character were investigated. The structure of product was confirmed by elemental analysis, IR and ()~1H NMR. |
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| Keywords: | 2 4-dichlorophenol phase-transfer catalyst orthogonal experiment 2-(2 4-dichlorophenoxy)triethylamine |
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