| 一种小分子敏感材料的制备与气敏特性研究 |
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| 引用本文： | 王晓杰,杜晓松,胡佳,黄嘉,蒋亚东.一种小分子敏感材料的制备与气敏特性研究[J].传感器与微系统,2011,30(11):62-64,68. |
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| 作者姓名： | 王晓杰 杜晓松 胡佳 黄嘉 蒋亚东 |
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| 作者单位： | 电子科技大学光电信息学院电子薄膜与集成器件国家重点实验室,四川成都,610054 |
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| 基金项目： | 国家自然科学基金资助项目(60876051,60736005); 教育部新世纪优秀人才支持计划资助项目(NECT-08-0086) |
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| 摘 要： | 合成了一种氢键酸性小分子神经毒气敏感材料.以二氯硅烷、2-溴甲基萘、活化锌粉、丙烯基苯为起始原料,通过格氏反应、硅氢加成,制备得到二(苯丙基)-二(2-萘基)甲基]硅烷,然后用六氟异丙醇进行取代,得到二3,5-双(2-羟基六氟异丙基)苯丙基]-二{(4,6,8-三3,5-双(2-羟基六氟异丙基)]-2-萘基)甲基...
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| 关 键 词： | 神经毒气 敏感材料 小分子 氢键酸性 声表面波传感器 |
Fabrication of small molecule sensitive material and study on gas sensitive charateristic |
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| WANG Xiao-jie,DU Xiao-song,HU Jia,HUANG Jia,JIANG Ya-dong.Fabrication of small molecule sensitive material and study on gas sensitive charateristic[J].Transducer and Microsystem Technology,2011,30(11):62-64,68. |
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| Authors: | WANG Xiao-jie DU Xiao-song HU Jia HUANG Jia JIANG Ya-dong |
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| Affiliation: | WANG Xiao-jie,DU Xiao-song,HU Jia,HUANG Jia,JIANG Ya-dong(State Key Laboratory of Electronic Thin Films and Integrated Devices,School of Optoelectronic Information,University of Electronic Science and Technology of China(UESTC),Chengdu 610054,China) |
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| Abstract: | A hydrogen bond acidic small molecule,bis3,5-bis(2-hydroxyhexafluoroisopropyl)phenpropyl]bis{4,6,8-tri3,5-bis(2-hydroxyhexafluoroisopropyl)]-2-naphthylmethyl}silane(HPNMS),is synthesized as sensitive material for nerve agents detection.Starting from dichlorosilane,2-(Bromomethyl)naphthalene,activated zinc and Allylbenzene,bisphenpropyl]bis{2-naphthylmethyl}silane is synthesized by Grignard reaction,hydrosilylation reaction and Reformatsky reaction.The intermediate product is functionalized by hexafluoroa... |
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| Keywords: | nerve agents sensitive material small molecule hydrogen-bond acidity surface acoustic wave(SAW)sensor |
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