45%氟菌·百菌清悬浮剂液相色谱定量分析 |
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引用本文: | 成妙金. 45%氟菌·百菌清悬浮剂液相色谱定量分析[J]. 世界农药, 2016, 0(2): 48-51. DOI: 10.16201/j.cnki.cn31-1827/tq.2016.02.13 |
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作者姓名: | 成妙金 |
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作者单位: | 深圳诺普信农化股份有限公司,广东深圳,518102 |
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摘 要: | 建立了在同一色谱条件下测定混剂中氟吡菌胺和百菌清含量的方法。采用250 min×4.60 mm(i.d.)Acclaim~(TM)120 C_(18)、5μm柱分离,以乙腈-水(体积比为70:30)为流动相,在210nm紫外检测波长下,经保留时间定性确证,峰面积外标法进行定量分析。百菌清与氟吡菌胺的线性相关系数分别为0.999 8和1.000 0;变异系数分别为0.37%和0.38%:平均回收率分别为99.48%和99.36%。该方法操作简便快捷,准确度和精密度高,线性相关性好,是较理想的分析方法。
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关 键 词: | 氟吡菌胺 百菌清 液相色谱 |
Analysis of Fluopicolide and Chlorothalonilin 45% SC by LC |
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Abstract: | A LC method for the determination of fluopicolide and chlorothalonil under the same chromatogram condition was developed. The LC conditions were AcclaimTM120 C18、5 μm column, acetonitrile-water (70:30 byvol) as mobile phage, and detection wave length at 210 nm. The results demonstrated that the correlation coefficients of chlorothalonil and fluopicolide were 0.999 8 and 1.000 0. The variation coefficients were 0.37% and 0.38%. The average recoveries were 99.48% and 99.36%. The method is simple, rapid, accurate and suitable for analysis of this kind of multiplex confected preparation. |
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Keywords: | fluopicolide chlorothalonil LC |
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