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敌稗在稻田环境中的残留动态
引用本文:金雅慧,郑尊涛,施海燕,王鸣华.敌稗在稻田环境中的残留动态[J].农药,2011,50(9).
作者姓名:金雅慧  郑尊涛  施海燕  王鸣华
作者单位:1. 南京农业大学植物保护学院,南京,210095
2. 农业部农药检定所,北京,100026
摘    要:目的]建立了敌稗在稻田环境中的残留检测方法.方法]样品经乙腈提取,液液分配后,气相色谱-电子捕获(ECD)法测定.结果]方法对敌稗在田水、土壤、植株、稻米和稻壳中的平均添加回收率为84.6%~105.5%,相对标准偏差1.0%~12.5%.敌稗在水稻田水、土壤、植株中的半衰期分别为0.9~2.9、0.7~2.0、1.0~1.3 d;在收获期土壤、植株、稻米、稻壳中敌稗的残留量均小于最低检测质量浓度.结论]该方法操作简单、快速,灵敏度高,符合农药残留分析的技术要求.

关 键 词:敌稗  水稻  残留动态

Residue Dynamics of Propanil in Rice Field Environment
JIN Ya-hui , ZHENG Zun-tao , SHI Hai-yan , WANG Ming-hua.Residue Dynamics of Propanil in Rice Field Environment[J].Pesticides,2011,50(9).
Authors:JIN Ya-hui  ZHENG Zun-tao  SHI Hai-yan  WANG Ming-hua
Affiliation:JIN Ya-hui1,ZHENG Zun-tao2,SHI Hai-yan1,WANG Ming-hua1(1.College of Plant Protection,Nanjing Agricultural University,Nanjing 210095,China,2.Institute for the Control of Agrochemicals,Ministry of Agriculture,Beijing 100026,China)
Abstract:The aim was to establish a method for the determination of propanil in rice field environment.Methods] Propanil were extracted from samples with acetonitrile and determined with GC-ECD after liquid-liquid partition.Results] The results indicated that the average recoveries of propanil spiked in water,soil,straw,rice,and bran samples ranged from 84.6-105.5%.And the relative standard deviation was 1.0-12.5%.The half-lives of degradation of propanil was 0.9-2.9 d in paddy water,0.7-2.0 d in paddy soil and 1....
Keywords:propanil  rice  residual dynamics  
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