| 4-[3-(4-氨基苯氧基)苯氧基]苯胺的合成研究 |
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| 引用本文： | 姚跃良,万佳韵.4-[3-(4-氨基苯氧基)苯氧基]苯胺的合成研究[J].化学世界,2007,48(4):228-231. |
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| 作者姓名： | 姚跃良 万佳韵 |
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| 作者单位： | 上海应用技术学院化学工程系,上海,200235 |
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| 摘 要： | 以间苯二酚和对硝基氯化苯为原料经醚化和水合肼还原合成了聚酰亚胺的二胺单体4-3-(4-氨基苯氧基)苯氧基]苯胺,总收率为79.8%,HPLC面积归一法测定目的产物为99.56%。并用元素分析和红外光谱对产物进行了表征。
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| 关 键 词： | 聚酰亚胺 4-[3-(4-氨基苯氧基)苯氧基]苯胺 醚化 水合肼还原 |
| 文章编号： | 0367-6358（2007）04-228-04 |
| 修稿时间： | 2006-04-012006-05-10 |
Synthesis of 4-[3-(4-Aminophenoxy) phenoxy ] phenylamine |
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| YAO Yue-liang,FAN Jia-yun.Synthesis of 4-[3-(4-Aminophenoxy) phenoxy ] phenylamine[J].Chemical World,2007,48(4):228-231. |
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| Authors: | YAO Yue-liang FAN Jia-yun |
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| Affiliation: | Department of Chemical Engineering, Shanghai Institute of Technology, Shanghai 200235, China |
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| Abstract: | A monomer of polyimide 4-3-(4-aminophenoxy)phenoxy] phenylamine was prepared from resorcinol and p-chloronitrobenzene through etherification reaction and hydrazine hydrate reduction with an overall yield of(79.8%).Its peak area was(99.56%) of the total peak area measured by HPLC area normalization method.The structure of the product was characterized by elemental analysis and FT IR spectroscopy. |
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| Keywords: | polyimide 4-[3-(4-aminophenoxy)phenoxy] phenylamine etherification reaction hydrazine hydrate reduction |
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