Accurate structure determination from image reconstruction in ADF STEM |
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Authors: | P. D. Nellist,& S. J. Pennycook |
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Affiliation: | Cavendish Laboratory, University of Cambridge, Madingley Road, Cambridge CB3 0HE, UK,;Oak Ridge National Laboratory, Solid State Division, PO Box 2008, Oak Ridge, TN 37831–6030, U.S.A. |
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Abstract: | Annular dark-field (ADF) imaging in a scanning transmission electron microscope results in direct structure images of the atomic configuration of the specimen. Since such images are almost perfectly incoherent they can be treated as a convolution between a point-spread function, which is simply the intensity of the illuminating electron probe, and a sharply peaked object function that represents the projected structure of the specimen. Knowledge of the object function for an image region of perfect crystal allows the point-spread function to be directly determined for that image. We examine how the object function for an image can then be reconstructed using a Wiener filter, the CLEAN algorithm and a maximum entropy reconstruction. Prior information is required to perform a reconstruction, and we discuss what nature of prior information is suitable for ADF imaging. |
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Keywords: | ADF image reconstruction incoherent imaging probe reconstruction STEM structure determination. |
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