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Novel Microwave-Assisted Synthesis of Renewable-Resource Based Carbon-Magnetite Nanocomposites
Authors:Chris Finlay  Gunawan Gunawan  Alexandru S Biris  Shawn Bourdo  Vasyl Kunets  Greg Salamo
Affiliation:1. Department of Chemistry , University of Arkansas at Little Rock , Little Rock , Arkansas , USA;2. Nanotechnology Center , University of Arkansas at Little Rock , Little Rock , Arkansas , USA;3. Department of Physics , University of Arkansas , Fayetteville , Arkansas , USA
Abstract:Abstract

Magnetic carbon-iron oxide nanoparticles have been synthesized using tannin, a renewable resource material, in combination with a microwave-based thermolytic process without the addition of any inert or reducing gas during the synthesis. The predominant iron oxide species present in these particles has been determined by XRD and FT-IR to be magnetite (Fe3O4). These iron oxide nanoparticles are embedded within a carbon matrix in small clusters generally ≤100 nm in size. The resulting powder is approximately 48% (w/w) magnetite, and has been characterized by magnetic susceptibility and SQUID analysis.
Keywords:Nanocomposite  magnetite  magnetic  nanoparticle  microwave  tannin  renewable  iron oxide
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