Novel Microwave-Assisted Synthesis of Renewable-Resource Based Carbon-Magnetite Nanocomposites |
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Authors: | Chris Finlay Gunawan Gunawan Alexandru S. Biris Shawn Bourdo Vasyl Kunets Greg Salamo |
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Affiliation: | 1. Department of Chemistry , University of Arkansas at Little Rock , Little Rock , Arkansas , USA;2. Nanotechnology Center , University of Arkansas at Little Rock , Little Rock , Arkansas , USA;3. Department of Physics , University of Arkansas , Fayetteville , Arkansas , USA |
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Abstract: | Abstract Magnetic carbon-iron oxide nanoparticles have been synthesized using tannin, a renewable resource material, in combination with a microwave-based thermolytic process without the addition of any inert or reducing gas during the synthesis. The predominant iron oxide species present in these particles has been determined by XRD and FT-IR to be magnetite (Fe3O4). These iron oxide nanoparticles are embedded within a carbon matrix in small clusters generally ≤100 nm in size. The resulting powder is approximately 48% (w/w) magnetite, and has been characterized by magnetic susceptibility and SQUID analysis. |
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Keywords: | Nanocomposite magnetite, magnetic nanoparticle microwave tannin renewable iron oxide |
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