A headspace solid-phase microextraction method development and its application in the determination of volatiles in honeys by gas chromatography |
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Authors: | Beata Plutowska Tomasz ChmielTomasz Dymerski Waldemar Wardencki |
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Affiliation: | Department of Analytical Chemistry, Chemical Faculty, Gdansk University of Technology, ul. Narutowicza 11/12, 80-233 Gdańsk, Poland |
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Abstract: | The first part of the paper presents the detailed optimisation of all steps of the determination procedure of volatiles from Polish honeys by headspace solid-phase microextraction (HS-SPME) as the sample preparation method and gas chromatography/mass spectrometry (GC–MS) as the method of final determination. In the result, the following conditions were applied: CAR/PDMS/DVB SPME fibre, the sample composition (5:1 w/w honey to water ratio), 3 g sample size. The other procedure parameters, like the temperatures of individual stages of the process, were also included. |
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Keywords: | Volatile compounds Aroma Honeys Solid-phase microextraction |
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