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Preparation of ZrO2 beads by an improved micro-droplet spray forming process
Authors:Jun Chen  Wan-Qing Xue  Chang-Ming Xu  Pai-Feng Luo  Ji-Gui Cheng  Ying-Wei Lu
Affiliation:1. School of Materials Science and Engineering, Hefei University of Technology, Hefei, P. R. China;2. Suzhou Nutpool Materials Technology Co., Ltd, Suzhou, P. R. China

Jiangxi Nutpool Industrial Co., Ltd, Yongfeng, P. R. China;3. School of Materials Science and Engineering, Hefei University of Technology, Hefei, P. R. China

Research Centre for Powder Metallurgy Engineering and Technology of Anhui Province, Hefei, P. R. China

Abstract:Monodisperse ZrO2 ceramic beads with size larger than 1 mm have been prepared by an improved micro-droplet spray forming process, through which a compressor and a dispenser were employed to produce droplets continuously. Furthermore, the slurry recipe and drying temperature have been optimized to enhance the sphericity and smoothness of the beads. The sintered ZrO2 ceramic beads present promising mechanical performance, including a relative density of 84.6%, a crush strength of 256.2 ± 36.6 N as well as a Vickers hardness of 1344.4 ± 58.3 HV. Such procedure reveals great potential in mass production of ceramic beads.
Keywords:mechanical performance  micro-droplet spray forming  optimization  ZrO2 beads
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