| 2,7-二溴-9-二烷硫基亚叉芴的合成及表征 |
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| 引用本文： | 李征,金玉子.2,7-二溴-9-二烷硫基亚叉芴的合成及表征[J].化学试剂,2009,31(12). |
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| 作者姓名： | 李征 金玉子 |
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| 作者单位： | 延边大学,理学院,化学系,吉林,延吉,133002 |
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| 摘 要： | 以芴为起始原料,合成了2,7-二溴-9-二甲硫基亚叉芴、2,7-二溴-9-二十二烷硫基亚叉芴、2,7-二溴-9-二苄硫基亚叉芴和2,7-二溴-9-二硫代乙烯撑亚叉芴4种新的芴衍生物.所得产物的结构经IR,NMR表征.
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| 关 键 词： | 芴衍生物 二硫缩烯酮 有机合成 |
Synthesis and characterization of ((2,7-dibromo-9H-fluoren-9-ylidene)methylene)bis(alkylsulfane) |
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| LI Zheng,JIN Yu-zi.Synthesis and characterization of ((2,7-dibromo-9H-fluoren-9-ylidene)methylene)bis(alkylsulfane)[J].Chemical Reagents,2009,31(12). |
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| Authors: | LI Zheng JIN Yu-zi |
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| Abstract: | Four new derivatives of fluorene-((2,7-dibromo-9H-fluoren-9-ylidene) methylene)bis(methylsulfane),((2,7-dibromo-9H-fluoren-9-ylidene)methylene)bis(dodecylsulfane),((2,7-dibromo-9H-fluoren-9-ylidene) methylene) bis(benzylsulfane) and 2-(2,7-dibromo-9H-fluoren-9-ylidene)-1,3-dithiolane were synthesized from the starting material fluorene.The structures of the target products were characterized by IR and NMR. |
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| Keywords: | fluorene derivatives ketene dithioacetal organic synthesis |
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