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原子吸收分光光度法测定磷酸锆银钠中的银
引用本文:陈小兰. 原子吸收分光光度法测定磷酸锆银钠中的银[J]. 广东有色金属学报, 2003, 13(1): 73-75
作者姓名:陈小兰
作者单位:广州有色金属研究院分析测试中心 广东
摘    要:先用硝酸 氢氟酸溶解磷酸锆银钠样品,再加氨水(1 1)使其转换成氨性溶液,然后用原子吸收分光光度法测定磷酸锆银钠中的银.本法测定结果与火试金法测定结果一致,相对标准偏差小于0.37%,回收率大于95%.

关 键 词:磷酸锆银钠 抗菌剂 银 原子吸收分光光度法 测定

Determination of silver in Ag_xNa_yH_(1-x-y)Zr_2(PO_4)_3 by atomic absorption spectrophotometry
CHEN Xiao-lan Analytical and Testing Research Center,Guangzhou Research Institute of Non-ferrous Metals,Guangzhou ,China. Determination of silver in Ag_xNa_yH_(1-x-y)Zr_2(PO_4)_3 by atomic absorption spectrophotometry[J]. Journal of Guangdong Non-Ferrous Metals, 2003, 13(1): 73-75
Authors:CHEN Xiao-lan Analytical  Testing Research Center  Guangzhou Research Institute of Non-ferrous Metals  Guangzhou   China
Affiliation:CHEN Xiao-lan Analytical and Testing Research Center,Guangzhou Research Institute of Non-ferrous Metals,Guangzhou 510651,China
Abstract:Ag_xNa_yH_(1-x-y)Zr_2 (PO_4)_3 is firstly dissolved into nitric acid and hydrofluoric acid,then ammonia water(1+1) is added to convert the resultant into ammoniac solution. Finallythe silver from Ag_xNa_yH_(1-x-y)Zr_2 (PO_4)_3 is determined by atomic absorption spectropho-tometry. The results from this method are in conformity with those from the fire assaying,with the relative standard deviation less than 0. 37% and the recovery over 95%.
Keywords:Ag_xNa_yH_1-x-yZr_2(PO_4)_3  silver  atomic absorption spectrophotometry
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