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石墨炉原子吸收法测定燃料油中金属钒
引用本文:陈信悦,孙延伟,于孝展,杨春光. 石墨炉原子吸收法测定燃料油中金属钒[J]. 精细石油化工, 2002, 0(2): 57-58
作者姓名:陈信悦  孙延伟  于孝展  杨春光
作者单位:辽宁出入境检验检疫局技术检验中心,大连,116001
摘    要:将试样在坩埚内燃烧 ,灰化后 ,用盐酸溶解 ,用石墨炉原子吸收法测定钒含量。实验表明 ,该法回收率98%~ 1 0 2 % ,能满足日常检验钒含量在 0~ 1 0 0 μg/g范围内的要求

关 键 词:燃料油  钒卟啉化合物  原子吸收光谱法  偏钒酸铵
修稿时间:2001-04-18

DETERMINATION OF METALLIC VANADIUM CONTENT IN FUEL OIL BY GRAPHITIC FURNACE ATOMIC ABSORPTION SPECTROSCOPY
Chen Xinyue,Sun Yanwei,Yu Xiaozhan and Yang Chunguang. DETERMINATION OF METALLIC VANADIUM CONTENT IN FUEL OIL BY GRAPHITIC FURNACE ATOMIC ABSORPTION SPECTROSCOPY[J]. Speciality Petrochemicals, 2002, 0(2): 57-58
Authors:Chen Xinyue  Sun Yanwei  Yu Xiaozhan  Yang Chunguang
Abstract:The samples were burnt in the crucible and ashed in the furnace at 600 ℃, dissolve the residue in HCL to make a solution for testing, then determine the vanadium in the fuel oil using graphitic furnace Atomic absorption spectroscopy. The testing results indicated that the recovery ratio is 98%102%. This method can satisfy the requirement of everyday tests while the vanadium content is in the range of 0100 μg/g.
Keywords:fuel oil  vanadium porphin compounds  atomic absorption spectroscopy  ammonium metavanadate  
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