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N-甲基吡咯烷酮生产分离系统的模拟计算与优化
引用本文:李钰,许朝阳,王祖元,崔鹏.N-甲基吡咯烷酮生产分离系统的模拟计算与优化[J].应用化工,2012,41(2):369-372.
作者姓名:李钰  许朝阳  王祖元  崔鹏
作者单位:1. 合肥工业大学化工学院,安徽合肥,230009
2. 安徽省化工设计院,安徽合肥,230009
摘    要:应用化工流程模拟软件Aspen Plus对N-甲基吡咯烷酮生产工艺中的分离系统进行模拟,将脱轻塔和脱重塔的操作方式由间歇操作改为连续操作,并对连续操作的脱轻塔和脱重塔的塔板数、进料位置、回流比等操作参数进行了优化。结果表明,优化的脱轻塔和脱重塔的适宜塔板数、进料板位置、最佳回流比分别为10,6,0.10和18,11,0.375。在此条件下,产品纯度达到99.40%,符合分离要求。

关 键 词:N-甲基吡咯烷酮  ASPENPLUS  模拟  脱轻塔  脱重塔

Simulation and optimization of separation system for production of N-methyl pyrrolidone
LI Yu , XU Zhao-yang , WANG Zu-yuan , CUI Peng.Simulation and optimization of separation system for production of N-methyl pyrrolidone[J].Applied chemical industry,2012,41(2):369-372.
Authors:LI Yu  XU Zhao-yang  WANG Zu-yuan  CUI Peng
Affiliation:1 (1.School of Chemical Engineering,Hefei University of Technology,Hefei 230009,China;2.Anhui Institute of Chemical Engineering Design,Hefei 230009,China)
Abstract:ASPEN PLUS was used to simulate the separation system for the production of N-methyl pyrrolidone.The operation mode of de-light rectifying column and de-heavy rectifying column were changed from batch operation into continuous operation.The stage number,feed stage and reflux ratio of de-light rectifying column and de-heavy rectifying column were also optimized,the results of which were 10,6,0.10 and 18,11,0.375,respectively.The product purity could reach 99.40% on the condition of optimized working conditions,and met with separation requirements.
Keywords:N-methyl pyrrolidone  Aspen Plus  simulation  de-light rectifying column  de-heavy rectifying column
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