| 马来酸催化改性木质素基染料分散剂的制备 |
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| 引用本文： | 刘志鹏,吴宜锴,刘明华.马来酸催化改性木质素基染料分散剂的制备[J].纤维素科学与技术,2013(4):23-30. |
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| 作者姓名： | 刘志鹏 吴宜锴 刘明华 |
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| 作者单位： | [1]福州大学环境与资源学院,福建福州350108 [2]福建省生物质资源化技术开发基地,福建福州350108 |
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| 基金项目： | 福建省企业技术创新专项项目;福建省生物产业技术开发项目. |
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| 摘 要： | 以马尾松木质素为原料，以马来酸为催化剂，制备改性木质素基染料分散剂（MLS），并通过正交单因素实验，对反应条件进行优化。实验结果表明，在磺化剂的用量为11％、甲醛用量为3．7％、20％硫酸用量为9％、马来酸用量为0．65％、羟甲基化时间为40min、羟甲基化温度为103℃、磺化时间为120min的条件下，分散等级4．7。
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| 关 键 词： | 木质素 染料分散剂 分散等级 制备 |
Preparation of Modified Lignin-Based Dye Dispersant by Maleic Acid Catalyzation |
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| LIU Zhi-peng,WU Yi-kai,LIU Ming-hua.Preparation of Modified Lignin-Based Dye Dispersant by Maleic Acid Catalyzation[J].Journal of Cellulose Science and Technology,2013(4):23-30. |
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| Authors: | LIU Zhi-peng WU Yi-kai LIU Ming-hua |
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| Affiliation: | . ( 1. College of Environment ＆ Resources, Fuzhou University, Fuzhou 350108, China; 2. Fujian Provincial Technology Exploitation Base of Biomass Resources, Fuzhou 350108, China) |
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| Abstract: | Modified lignin-based dye dispersant （MLS） was prepared using ligin as raw material and maleic acid as catalyst. The preparation conditions were optimized by orthogonal and signal-factor experiments. And the results concluded that the optimum conditions were 11% of sulfonating agent, 3.7% of formaldehyde, 9% of 20% sulfuric acid, 0.65% of maleic acid, 40 min of hydroxyl methylation time, 103°C of hydroxyl methylation temperature, and 120 min of sulfonated time. Under the optimal conditions, the dispersion level of the lignin-based dye dispersant could reach 4.7. |
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| Keywords: | lignin dye dispersant dispersion level preparation |
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