| 疏水单体叔丁基丙烯酰胺的合成 |
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| 引用本文： | 刘冬根,汪海波,李绵贵,王兆惠.疏水单体叔丁基丙烯酰胺的合成[J].云南化工,2006,33(5):27-28,40. |
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| 作者姓名： | 刘冬根 汪海波 李绵贵 王兆惠 |
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| 作者单位： | 湖北省化学研究院,湖北,武汉,430047 |
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| 摘 要： | 用叔丁胺与丙烯酰氯胺解法合成了疏水单体叔丁基丙烯酰胺，其结构及纯度用IR和GC进行了表征。考察了丙烯酰氯与叔丁胺的物质的量比及反应时间对产物收率的影响，结果表明丙烯酰氯与叔丁胺的物质的量比为1：1．4，反应时间4h，收率可达74％，纯度99．16％。
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| 关 键 词： | 疏水单体 疏水缔合聚合物 叔丁基丙烯酰胺 合成 |
| 文章编号： | 1004-275X（2006）05-0027-02 |
| 收稿时间： | 2006-06-26 |
| 修稿时间： | 2006-06-26 |
Synthesis of hydrophobic momomer N-tert-butyl acrylamide |
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| LIU Dong-gen,WANG Hai-bo,LI Mian-gui,WANG Zao-hui.Synthesis of hydrophobic momomer N-tert-butyl acrylamide[J].Yunnan Chemical Technology,2006,33(5):27-28,40. |
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| Authors: | LIU Dong-gen WANG Hai-bo LI Mian-gui WANG Zao-hui |
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| Affiliation: | Hubei Research Institute of Chemistry , Wuhan 430074, China |
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| Abstract: | N-tert-butyl acrylamide was synthesized by the reaction of acryloyl chloride with n-tert-butylamine , the structure and purity was determined by IR and GC. The effect of ratio and reaction time on yield were investigated. At the same ratio, the long reaction time , the higher yield. Finally , we get a product with the yield of 74% and purity of 99.12%. |
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| Keywords: | hydrophoblc monomer hydrophobie associated polymer N-ten-butyl aerylamide synthesis |
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