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鸢尾中鸢尾酮的气相色谱-质谱联机分析
引用本文:郭涛,杨克迪,陈钧. 鸢尾中鸢尾酮的气相色谱-质谱联机分析[J]. 食品科学, 2005, 26(1): 172-176
作者姓名:郭涛  杨克迪  陈钧
作者单位:江苏大学生物与环境工程学院,江苏,镇江,212013
基金项目:中国烟草总公司云南省公司项目(2001(B)203)
摘    要:目的:建立鸢尾原料中鸢尾酮含量的分析方法。方法:采用气相色谱-质谱法定性鉴定鸢尾酮的三种异构体,气相色谱外标法定量分析鸢尾酮的含量。结果:依据质谱裂解规律初步鉴定三种鸢尾酮的异构体,测定了两批原料中鸢尾酮的含量。结论:采用气相色谱-质谱法及气相色谱法分析鸢尾酮,简便、高效、准确、分析时间适中。

关 键 词:鸢尾酮 气相色谱法 气相色谱-质谱法
文章编号:1002-6630(2005)01-0172-05

Analysis of Irone in Iris Tectorum by GC/MS
GUO Tao,YANG Ke-di,CHEN Jun. Analysis of Irone in Iris Tectorum by GC/MS[J]. Food Science, 2005, 26(1): 172-176
Authors:GUO Tao  YANG Ke-di  CHEN Jun
Abstract:Objective: To establish a method for determination of Irone in Iris tectorum. Method: The three isomers of Irone were quantitatively analyzed by GC-MS. Irone in Iris tectorum was determinated according to the extra-calibration curve by GC. Results: The three isomers of irone was speculated according to the MS _ splitting _decomposition law. Irone in two passel of Iris tectorum material was determinated. Conclusion: The analysis method for irone using GC-MS and GC was high- efficient, precise. The analysis time was acceptable.
Keywords:Irone  GC  GC-MS
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