固定床吸附柱放大效应考察─—理论板当量高度分析 |
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引用本文: | 叶振华,吴启龙.固定床吸附柱放大效应考察─—理论板当量高度分析[J].化学工程,1994,22(4):25-29,41. |
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作者姓名: | 叶振华 吴启龙 |
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摘 要: | 从色谱塔板理论公式出发,推导出实测理论板公式及理论极当量高度和吸附热力学、吸附动力学参数之间的关系,并对模型的选择、优化操作线速的选取作了讨论。实验测定了d_p/d_t=4.0/20.0时,吸附柱内的轴向扩散系数及流体传质系数,并加以关联。对不同压力、流量下的理论板当量高度也进行了检验。
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关 键 词: | 固定床吸附柱,放大效应,理论板当量高度 |
SCALE-UP EFFECT OF FIXED ADSORPTION COLUMN HEIGHT EQUIVALENT TO A THEORETICAL PLATE |
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Abstract: | ased on the theoratical formula for chromatographic plate,the formula for measuring the experi-mental height equivalent to a theoretical plate(HETP)is derived,and the relationship between HETPand the parameters of adsorption thermodynamics and kinetics are also obtained.The selections of med-els,optimized oporation linear velocity are discussed.The axial diffusion coefficients and mass transfercoefficients are measured exporimentally in an adsorption column(dp/dt=4.0/20.0),and the corre-lation of the above coefficients is carried out.Finally, HETP is checked for the values at different pres-sure and flowrate. |
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Keywords: | Scale-up effect of fixed adsorption column HETP |
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