Effect of cooling rate on the 3D morphology of the proeutectic Al_3Ni intermetallic compound formed at the Al/Ni interface after solidification |
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Authors: | Liao Yu Qiaodan Hu Zongye Ding Fan Yang Wenquan Lu Naifang Zhang Sheng Cao Jianguo Li |
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Abstract: | Effect of cooling rate on the 3 D morphology and the growth mechanism of the proeutectic Al_3Ni intermetallic compound(IMC) that forms at the Al/Ni interface after solidification was investigated by synchrotron X-ray microtomography in combination with EBSD analysis. The proeutectic Al_3Ni phase that forms under an average cooling rate of 0.1 Ks~(-1) shows a characteristic faceted growth behavior and presents a typical 3 D morphology as partially hollow quadrangular prisms. On the contrary, that forms under an average cooling rate of 10 Ks~(-1) shows complicated dendritic morphology with asymmetrically distributed arms and faceted V-shape groove at the distal end, indicating a gradual transition of the growth behavior from non-faceted to faceted during the solidification process. These results reveal that the morphology of the proeutectic Al_3Ni is highly sensitive to the solidification condition so that fine control of the desired morphology may be achieved by carefully manipulating the cooling profile. |
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Keywords: | 3D morphology Al3Ni intermetallic compounds Solidification Cooling rate Synchrotron radiation Al/Ni interface |
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