| 脂肪醇在三(3,5-二硝基苯甲酸)纤维素酯固定相上的分离 |
| |
| 引用本文： | 施介华,李景华,杨根生,廖钟财,王建军.脂肪醇在三(3,5-二硝基苯甲酸)纤维素酯固定相上的分离[J].浙江工业大学学报,2003,31(1):88-91. |
| |
| 作者姓名： | 施介华 李景华 杨根生 廖钟财 王建军 |
| |
| 作者单位： | 浙江工业大学,药学院,浙江,杭州,310032 |
| |
| 摘 要： | 采用以苯甲酸和微晶纤维素等为基本原料通过硝化、酰氯化和催化酯化反应合成三（3，5－二硝基苯甲酸）纤维素酯，并将其负载于GDX103载体上，在其固定相上成功地分离C1－C6脂肪醇，特别是较好地分离丙醇和丁醇的六个异构体。
|
| 关 键 词： | 三（3 5－二硝基苯甲酸）纤维素酯 色谱固定相 脂肪醇 分离 |
| 文章编号： | 1006-4303(2003)01-0088-04 |
| 修稿时间： | 2002年3月5日 |
Separation of aliphatic alcohols on the chromatographic stationaryphase of cellulose tris (3,5-dinitrobenzoate) |
| |
| SHI Jie\|hua,LI Jing\|hua,YANG Gen\|sheng,LIAO Zhong\|cai,WANG Jian\|jun.Separation of aliphatic alcohols on the chromatographic stationaryphase of cellulose tris (3,5-dinitrobenzoate)[J].Journal of Zhejiang University of Technology,2003,31(1):88-91. |
| |
| Authors: | SHI Jie\|hua LI Jing\|hua YANG Gen\|sheng LIAO Zhong\|cai WANG Jian\|jun |
| |
| Abstract: | The cellulose tris (3,5\|dinitrobenzoate) was synthesised by nitrification, chloride acylation and catalytic esterification with the basic raw materials of benzoic acid, microcrystalline cellulose, etc. Then, cellulose tris (3,5\|dinitrobenzoate) was supported on GDX 103. The aliphatic alcohols (C\-1-C\-6) were successfully separated on the chromatographic stationary phase of the cellulose tris (3,5\|dinitrobenzoate), in particular, the separation of six isomers of propanol and butanol was achieved. |
| |
| Keywords: | cellulose tris (3 5\|dinitrobenzoate) chromatographic stationary phase aliphatic alcohol separation |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
