| 脂肪醇在三(3,5-二硝基苯甲酸)纤维素酯固定相上的分离 |
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| 引用本文： | 施介华,李景华,杨根生,廖钟财,王建军. 脂肪醇在三(3,5-二硝基苯甲酸)纤维素酯固定相上的分离[J]. 浙江工业大学学报, 2003, 31(1): 88-91 |
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| 作者姓名： | 施介华 李景华 杨根生 廖钟财 王建军 |
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| 作者单位： | 浙江工业大学,药学院,浙江,杭州,310032 |
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| 摘 要： | 采用以苯甲酸和微晶纤维素等为基本原料通过硝化、酰氯化和催化酯化反应合成三（3，5－二硝基苯甲酸）纤维素酯，并将其负载于GDX103载体上，在其固定相上成功地分离C1－C6脂肪醇，特别是较好地分离丙醇和丁醇的六个异构体。
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| 关 键 词： | 三（3 5－二硝基苯甲酸）纤维素酯 色谱固定相 脂肪醇 分离 |
| 文章编号： | 1006-4303(2003)01-0088-04 |
| 修稿时间： | 2002-03-05 |
Separation of aliphatic alcohols on the chromatographic stationaryphase of cellulose tris (3,5-dinitrobenzoate) |
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| SHI Jie|hua,LI Jing|hua,YANG Gen|sheng,LIAO Zhong|cai,WANG Jian|jun. Separation of aliphatic alcohols on the chromatographic stationaryphase of cellulose tris (3,5-dinitrobenzoate)[J]. Journal of Zhejiang University of Technology, 2003, 31(1): 88-91 |
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| Authors: | SHI Jie|hua LI Jing|hua YANG Gen|sheng LIAO Zhong|cai WANG Jian|jun |
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| Abstract: | The cellulose tris (3,5|dinitrobenzoate) was synthesised by nitrification, chloride acylation and catalytic esterification with the basic raw materials of benzoic acid, microcrystalline cellulose, etc. Then, cellulose tris (3,5|dinitrobenzoate) was supported on GDX 103. The aliphatic alcohols (C-1-C-6) were successfully separated on the chromatographic stationary phase of the cellulose tris (3,5|dinitrobenzoate), in particular, the separation of six isomers of propanol and butanol was achieved. |
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| Keywords: | cellulose tris (3 5|dinitrobenzoate) chromatographic stationary phase aliphatic alcohol separation |
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