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SHS-GC-MS分析黄酒中的挥发性风味物质
引用本文:王家林,苏海荣,于秦峰.SHS-GC-MS分析黄酒中的挥发性风味物质[J].中国酿造,2012,31(5):188-190.
作者姓名:王家林  苏海荣  于秦峰
作者单位:1. 青岛科技大学生物工程与技术系,山东青岛,266042
2. 妙府老酒有限公司,山东青岛,266042
基金项目:校企合作项目(20103702001014)
摘    要:采用自动静态顶空进样技术,结合气质联用对黄酒中的挥发性风味物质进行分析.通过单因素水平实验得到优化的顶空条件:在10mL顶空瓶中加入样品5mL,NaC1 2.0g,60℃萃取30min.通过GC-MS分析,初步确定了26种风味成分,其中大部分为酯类和醇类.

关 键 词:黄酒  挥发性风味物质  静态顶空(SHS)  气相色谱—质谱

Characterization of volatile compounds in Chinese rice wine by static headspace-gas chromatography-mass spectrometry
WANG Jialin , SU Hairong , YU Qinfeng.Characterization of volatile compounds in Chinese rice wine by static headspace-gas chromatography-mass spectrometry[J].China Brewing,2012,31(5):188-190.
Authors:WANG Jialin  SU Hairong  YU Qinfeng
Affiliation:1.Department of Bioengineering and Technology,Qingdao University of Science & Technology,Qingdao 266042,China;2.Miaofu Rice Wine Co.,Ltd.,Qingdao 266042,China)
Abstract:The volatile compounds in Chinese rice wine were analyzed by static headspace-gas chromatography-mass spectrometry.The headspace conditions were optimized by single factor experiments as follows: 5ml sample in 10ml vial,2.0g NaCl,extraction time 30min and extraction temperature 60℃.A total of 26 compounds were detected and identified by GC-MS,and most of them were esters and alcohols.
Keywords:rice wine  volatile compounds  static headspace(SHS)  gas chromatography-mass spectrometry(GC-MS)
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