Ion reduction in iron oxide and oxyhydroxide nanoparticles during ultrasonic treatment |
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Authors: | SV Stolyar OA Bayukov RN Yaroslavtsev YuV Knyazev VP Ladygina YuV Gerasimova RS Iskhakov |
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Affiliation: | 1. Siberian Federal University, Krasnoyarsk, Russia;2. Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, Russia;3. Krasnoyarsk Scientific Center, Federal Research Center KSC SB RAS, Krasnoyarsk, Russia |
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Abstract: | The effect of ultrasonic treatment of iron oxide and iron oxyhydroxide nanoparticles (ferrihydrite nanoparticles synthesized by Klebsiella oxytoca microorganisms, ferrihydrite nanoparticles synthesized by a chemical method and hematite nanoparticles) is studied. Samples of nanoparticles were investigated using transmission electron microscopy, Mössbauer spectroscopy and X-ray diffraction methods. The formation of the α-Fe metal phase from nanoparticles of iron oxides and iron oxyhydroxides was detected. The metal phase is formed as a result of the reduction of iron ions during cavitation treatment. According to the experimental results, the presence of a protein or a polysaccharide component is necessary for the course of this reaction. |
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Keywords: | Corresponding author Nanoparticles Ferrihydrite Ultrasonic cavitation |
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