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Dispersion of carbon nanofibres in a low viscosity resin by calendering process to manufacture multiscale composites by VARIM
Authors:A. Jiménez-Suárez  M. Campo  M. Sánchez  C. Romón  A. Ureña
Affiliation:1. Institute of Aircraft Design, University of Stuttgart, Pfaffenwaldring 31, 70569 Stuttgart, Germany;2. ARENA2036 Research Campus, Pfaffenwaldring 19, 70569 Stuttgart, Germany;3. Henkel Ireland Operations and Research Ltd., Tallaght, Dublin 24, Ireland;1. Key Laboratory of Bioelectronics (Chien-Shiung Wu Lab), School of Biological Science and Medical Engineering, Southeast University, Nanjing 210096, China;2. Nanjing Tenyi High-tech Materials Co., Ltd, Nanjing 210048, China;3. AutoX Co., Ltd, Shenzhen 518052, China;4. Hunan Key Laboratory of Biomedical Nanomaterials and Devices, Hunan University of Technology, Zhuzhou 412007, China;1. ESIME Azcapotzalco, Instituto Politécnico Nacional, Av. de las Granjas No. 682, Col. Santa Catarina, Del. Azcapotzalco, Mexico D.F. 02250, Mexico;2. Departamento de Termofluidos, Facultad de Ingeniería, UNAM, Mexico D. F. 04510, Mexico;1. Institute of Advanced Composite Materials, Korea Institute of Science and Technology (KIST), 92 Chudong-ro, Bongdong-eup, Wanju-gun, Jeonbuk, 55324, Republic of Korea;2. School of Materials Science and Engineering, Gwangju Institute of Science and Technology (GIST), 123 Cheomdangwagi-ro, Buk-gu, Gwangju, 61005, Republic of Korea;3. Department of Organic and Nano System Engineering, Konkuk University, Seoul, 05029, Republic of Korea;4. Global Aqua Innovation Center, and Institute of Carbon Science and Technology, Faculty of Engineering, Shinshu University, Nagano City, 380-8553, Japan;5. School of Polymer Science and Engineering, Chonnam National University, 77 Yongbong-ro, Buk-gu, Gwangju, 61186, Republic of Korea
Abstract:The use of mechanical processes, such as calendering, is an interesting method to disperse carbon nanofibres because this technique avoids the use of organic solvents needed in chemical methods. Variations of the process are used by researchers, and further study of the effect of the calendering parameters is still needed. For this reason, the effectiveness of the dispersion of several percentages of carbon nanofibres (0.5–3 wt.%) in epoxy resin using different parameters of the calendering process has been studied in this work. Carbon nanofibres/epoxy nanocomposites and non-cured nanoreinforced mixtures have been characterised. This study showed that the dispersion was enhanced with a Sequential method. Density and thermomechanical properties of nanocomposites manufactured by the selected calendering method were evaluated. The viscosity of the CNF/epoxy mixtures at different percentages of nanoreinforcement was adequate to use them as a matrix in multiscale reinforced composites.
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