| HPLC测定丹黄祛瘀胶囊中丹参素钠的含量 |
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| 引用本文： | 谢世全,王巍,赵焕君. HPLC测定丹黄祛瘀胶囊中丹参素钠的含量[J]. 广州化工, 2012, 40(15): 157-158 |
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| 作者姓名： | 谢世全 王巍 赵焕君 |
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| 作者单位： | 辽宁中医药大学药学院,大连辽宁,116600 |
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| 摘 要： | 建立了丹黄祛瘀胶囊中丹参素钠的含量测定方法。采用Agilent C18柱(250 mm×4.6 mm,5μm),流动相为甲醇-0.1%磷酸(10∶95),柱温30℃,流速1.0 mL/min,检测波长280 nm。结果表明:丹参素钠在0.279～3.069μg内线性关系良好(r=0.9995);平均回收率为99.2%,RSD=0.87%(n=6),该法可用于控制丹黄祛瘀胶囊的质量。
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| 关 键 词： | 高效液相色谱法 丹黄祛瘀胶囊 丹参素钠 |
Determination of Sodium Danshensu in Danhuang Quyu Capsule by HPLC |
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| XIE Shi-quan,WANG Wei,ZHAO Huan-jun. Determination of Sodium Danshensu in Danhuang Quyu Capsule by HPLC[J]. GuangZhou Chemical Industry and Technology, 2012, 40(15): 157-158 |
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| Authors: | XIE Shi-quan WANG Wei ZHAO Huan-jun |
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| Affiliation: | (School of Pharmacy,Liaoning University of TCM,Liaoning Dalian 116600,China) |
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| Abstract: | To establish a HPLC method for determination of Sodium Danshensu in Danhuang Quyu capsule.An Agilent C18 column（4.6 nm×250 mm,5 μm） was used,the mobile phase was methanol-0.1% phosphoric acid（10：95）,the detection wavelength was 280 nm,the column temperatuer was 30 ℃ and the flow rate was 1.0 mL·min-1.Sodium Danshensu showed a good linear relationship in the range of was 0.279~3.069 μg（r=0.9995）,the average recovery was 99.2%,RSD=0.87%（n=6）.The method is accurate and reliable,it can be used for the quality control of Danhuang Quyu capsule. |
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| Keywords: | HPLC Danhuang Quyu capsule sodium danshensu |
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