固液相转移催化法合成一缩二乙二醇双丁醚 |
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引用本文: | 赵鸿斌 蔡德军. 固液相转移催化法合成一缩二乙二醇双丁醚[J]. 山东化工, 2000, 29(4): 3-4 |
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作者姓名: | 赵鸿斌 蔡德军 |
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作者单位: | 湘潭大学化学化工学院,湖南湘潭 |
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摘 要: | 采用固-液相转移催化的新方法,在氢氧化钾的存在下,一缩二乙二醇与溴代正丁烷反应合成一缩二乙二醇双丁醚。考察了催化剂的种类、催化剂的用量、溶剂、反应温度等对反应收率的影响。
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关 键 词: | 一缩二乙二醇双丁醚 固液相转移催化法 合成 |
Study on the Solid-liquid Phase Transfer Catalyzed Synthesis of Diethylene Glycol Dibutyl Ether |
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Abstract: | This paper reports that diethylene glycol reacts with potassium hydroxide and n-bromobutane to synthesize dibutyl ether by means of solid-liquid phase transfer catalysis.In the process of experiments,the influences of the varieties and the quantity of catalyst,the temperature,the solvents etc,are researched on the productivity. |
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Keywords: | phase transfer catalysis diethylene glycol diethylene glycol dibutyl |
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