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城市污水中总砷测定
引用本文:徐健. 城市污水中总砷测定[J]. 陶瓷科学与艺术, 2001, 0(2)
作者姓名:徐健
作者单位:南京市城市排水监测站!南京,210003
摘    要:用氢化物发生 -原子荧光光谱法测定城市污水中总砷 ,确定了试验的最佳测定条件。结果表明 :砷的测定线性范围为 5~ 5 0 ng/ m L,回收率 10 0 %~ 10 3% ,测定 6条标准曲线的剩余标准差为 1.3,检出限为 0 .2 6 ng/ m L,该方法可用于测定其它不同水体中的总砷。

关 键 词:氢化物发生-原子荧光光谱法  城市污水  微量分析  

DETERMINATION OF TOTAL ARSENIC IN CITY WASTE WATER
Xu Jian Nanjing Municipal Drainage Monitoring Center Nanjing,,China. DETERMINATION OF TOTAL ARSENIC IN CITY WASTE WATER[J]. Ceramics Science & Art, 2001, 0(2)
Authors:Xu Jian Nanjing Municipal Drainage Monitoring Center Nanjing    China
Affiliation:Xu Jian Nanjing Municipal Drainage Monitoring Center Nanjing,210003,China
Abstract:Determination of total arsenic in city waste water samples by hydride generation atomic fluorescence spectrometry was described.The optimum condition of determination was discussed.The linear range of determination was from 5 ng/mL to 50 ng/mL,recovery rate was 100%~103%,the residual standard deviation of six specification curves was 1.3 and the detection limit was 0.26 ng/mL. The method can be used to assay total arsenic in other different water samples.
Keywords:hydride generation atomic fluoresence spectrometry city waste water microanalysis arsenic  
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