| 3,3,3-三氟丙基甲基二甲氧基硅烷合成研究 |
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| 引用本文： | 廖洪流,朱淮军,李凤仪.3,3,3-三氟丙基甲基二甲氧基硅烷合成研究[J].化工新型材料,2005,33(12):36-38. |
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| 作者姓名： | 廖洪流 朱淮军 李凤仪 |
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| 作者单位： | 1. 华南理工大学化工学院,广州,510641
2. 南昌大学化学系,南昌,330047 |
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| 摘 要： | 通过滴加3,3,3-三氟丙基甲基二氯硅烷与甲醇进行醇解反应,合成了3,3,3-三氟丙基甲基二甲氧基硅烷,考察了不同的溶剂、温度、加料速度等对产物的影响,确立了最佳的反应条件。并用GC-MS对产物进行定量和定性分析。
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| 关 键 词： | 3 3 3-三氟丙基甲基二氯硅烷 3 3 3-三氟丙基甲基二甲氧基硅烷 甲醇 合成 醇解 |
| 修稿时间： | 2005年4月28日 |
Study on synthesis of 3,3,3-trifluoropropylmethyldimethoxysilane |
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| Liao Hongliu,Zhu Huaijun,Li Fengyi.Study on synthesis of 3,3,3-trifluoropropylmethyldimethoxysilane[J].New Chemical Materials,2005,33(12):36-38. |
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| Authors: | Liao Hongliu Zhu Huaijun Li Fengyi |
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| Affiliation: | Liao Hongliu~1 Zhu Huaijun~2 Li Fengyi~2 |
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| Abstract: | 3,3,3-Trifluoropropylmethyldimethoxysilane was synthesized by the alcoholysis reaction of trifluoropropylmethyldichlorosilane and methanol with solvent method.The effects of different solvents and reacting conditions such as temperature,adding material were studied. And the appropriate reaction condition were established.The composition of products were examined by GC-MS method. |
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| Keywords: | 3 3 3-trifluoropropylmethyldichlorosilane 3 3 3-trifluoropropylmethyldimethoxysilane methanol synthesis alcoholysis |
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