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响应面法优化超声波辅助提取豹皮樟多酚工艺
引用本文:张宇思,王成章,舒阿庆,叶建中.响应面法优化超声波辅助提取豹皮樟多酚工艺[J].生物质化学工程,2014(5):19-23.
作者姓名:张宇思  王成章  舒阿庆  叶建中
作者单位:1. 中国林业科学研究院林产化学工业研究所/生物质化学利用国家工程实验室/国家林业局林产化学工程重点开放性实验室/江苏省生物质能源与材料重点实验室,江苏 南京,210042
2. 中国林业科学研究院林产化学工业研究所/生物质化学利用国家工程实验室/国家林业局林产化学工程重点开放性实验室/江苏省生物质能源与材料重点实验室,江苏 南京 210042; 中国林业科学研究院林业新技术研究所,北京 100091
3. 宁国市亿邦生物科技有限公司,安徽 宁国,242300
基金项目:“十一五”国家科技支撑计划资助项目(2011BAD33B02);国际科技合作专项
摘    要:在单因素试验的基础上,选定提取时间、液固比、超声波功率为自变量,以多酚得率为响应值,采用Box-Benhnken法设计3因素3水平的响应面分析试验优化超声波辅助提取豹皮樟多酚工艺。结果表明,回归模型拟合度高,最佳工艺条件为:5 g样品,提取时间22 min,液固比21∶1(mL∶g,下同),超声波功率300 W,在此条件下,豹皮樟多酚得率可达3.76%。

关 键 词:豹皮樟  多酚  超声波辅助提取  响应面优化

Optimization of Ultrasonic-assisted Extraction of Polyphenol from Litsea Coreana using Response Surface Methodology
ZHANG Yu-si,WANG Cheng-zhang,SHU A-qing,YE Jian-zhong.Optimization of Ultrasonic-assisted Extraction of Polyphenol from Litsea Coreana using Response Surface Methodology[J].Biomass Chemical Engineering,2014(5):19-23.
Authors:ZHANG Yu-si  WANG Cheng-zhang  SHU A-qing  YE Jian-zhong
Affiliation:ZHANG Yu-si, WANG Cheng-zhang, SHU A-qing, YE Jian-zhong ( 1. Institute of Chemical Industry of Forest Products, CAF ; National Engineering Lab. for Biomass Chemical Utilization; Key and Open Lab. of Forest Chemical Engineering,SFA;Key Lab. of Biomass Energy and Material,Jiangsu Province, Nanjing 210042, China; 2. Research Institute of Forestry New Technology,CAF, Beijing 100091, China; 3. Ningguo Yibang Biotechnology Co. ,Ltd., Ningguo 242300, China)
Abstract:Based on single factor test,a 3-factor,3-level Box-Behnken experimental was adopted,including dependent variables ( extraction time,liquid-solid ratio and ultrasonic wave power ) and independent variable( polyphenol yield ). The optimum conditions of ultrasonic-assisted extraction technology for polyphenol from Litsea coreana were determined by using response surface method. The results showed that the regression model fitted well with experimental data. The optimum conditions were 5 g samples,extraction time 22 min,liquid-solid ratio 21:1,ultrasonic wave power 300 W. Under these conditions,the polyphenol yield was 3. 76%.
Keywords:Litsea coreana  polyphenol  ultrasonic-assisted extraction  response surface optimization
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