| 丁酸异戊酯合成工艺研究 |
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| 引用本文： | 植中强,蓝向荣,李红缨,杨海贵. 丁酸异戊酯合成工艺研究[J]. 化学工程师, 2004, 18(4): 8-9 |
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| 作者姓名： | 植中强 蓝向荣 李红缨 杨海贵 |
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| 作者单位： | 肇庆学院,轻工化学系,广东,肇庆,525061;肇庆市第十二中学,广东,肇庆,526020 |
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| 摘 要： | 以环己烷为带水剂，采用微波辐射技术，在对甲苯磺酸的催化下，快速合成了丁酸异戊酯。探讨了原料配比、反应时间、催化剂用量、微波功率等参数对酯化率的影响。在适宜工艺条件下，酯化率可达99％以上。
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| 关 键 词： | 微波 合成 对甲苯磺酸 丁酸异戊酯 |
| 文章编号： | 1002-1124(2004)04-0008-02 |
| 修稿时间： | 2004-03-01 |
Study on the synthesis of isoamyl butyrate |
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| ZHI Zhong-qiang ,LAN Xiang-rong ,LI Hong-ying ,YANG Hai-gui. Study on the synthesis of isoamyl butyrate[J]. Chemical Engineer, 2004, 18(4): 8-9 |
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| Authors: | ZHI Zhong-qiang LAN Xiang-rong LI Hong-ying YANG Hai-gui |
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| Affiliation: | ZHI Zhong-qiang 1,LAN Xiang-rong 2,LI Hong-ying 1,YANG Hai-gui 1 |
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| Abstract: | By using the technique of microwave radiation,under the catalysising of p -toluenesulfonic acid,cyclohexane as water entrainer,isoamyl butyrate can be synthesized fastly.Researches the influence of different parameters such as,the proportion of raw materials,the time of reaction,the dose of catalyst,the power of micarwave on the rate of esterification.Under the suitable technological conditions,the rate of esterification was over 99%. |
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| Keywords: | microwave synthesis p-toluenesulfonic acid isoamyl butyrate |
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