Synthesis and Characterization of Dialkyl-C61 |
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| Authors: | Masanori Kawasumi Takayuki Ishida Takashi Nogami |
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| Affiliation: |
a Tokyo Technical Research Laboratory, Mita Industrial Co., Ltd., Tokyo, Japan
b Department of Applied Physics and Chemistry, The University of Electro-Communications, Tokyo, Japan |
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| Abstract: | Three-step synthesis from dialkyl ketone (R2C=O) with C60 gave C60(CR2)n R = Me, Et, Pr, Bu, (CH2)5.; n = 1, 2]. The adducts were isolated by means of gel permeation chromatography, and the monoadducts were characterized by 1H and/or 13C NMR spectroscopies as a mixture of major 5, 6] and minor 6, 6] isomers. Their solubility and electrochemical properties were reported. |
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