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Neutron and X-ray reflectivity analysis of ceramic-metal materials
Authors:A. Gibaud   C. Sella   M. Maaza   L. Sung   J. A. Dura  S. K. Satija
Affiliation:

a Université du Maine, Faculté des Sciences, UPRESA 6087 CNRS, 72085 Le Mans Cedex 09, France

b Laboratoire d’Optique des Solides, Université de Paris VI, Tour 13, 75006 Paris, France

c Department of Physics, University of the Witswatersrand, P.O. Wits, Johannesburg, South Africa

d Materials Science and Engineering Laboratory, National Institute of Standards and Technology, Bld 235, Gaithersburg MD 20899-0001, USA

Abstract:Neutron and X-ray reflectivity measurements of a thin film of cermet (ceramic-metal) made by co-sputtering Pt and Al2O3 on the surface of a flat piece of float glass are presented. From the analysis of the specular and off-specular measurements, the morphology of the Pt clusters which are embedded in the Al2O3 matrix is determined by adjusting a model to the observed data. It is found that the structure of such films presents a certain degree of order in the direction normal to the surface of the films but no correlation (or with a very short correlation length not measurable by this technique) in the plane of the film.
Keywords:X-ray scattering   Platinum   Ceramic-metal   X-ray reflectivity
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