| N-甲基-2-吡咯腈的合成与表征 |
| |
| 引用本文： | 梁志宏,赵林,谢亚雄,朱雁,原思国. N-甲基-2-吡咯腈的合成与表征[J]. 河南化工, 2003, 0(11): 10-11 |
| |
| 作者姓名： | 梁志宏 赵林 谢亚雄 朱雁 原思国 |
| |
| 作者单位： | 1. 河南省精细化工重点实验室,河南,郑州,450002
2. 河南省分析测试中心,河南,郑州,450002 |
| |
| 基金项目： | 河南省杰出人才创新基金 ( 0 12 10 0 160 0 ) |
| |
| 摘 要： | 以N—甲基—2—吡咯醛为原料，经肟化、脱水合成了N—甲基—2—吡咯腈，通过气相色谱对产品纯度进行测定，并用红外光谱、质谱对其结构进行了表征。用二氯乙烷代替乙醚作萃取剂具有生产安全性好、溶剂损耗少、成本低等优点。
|
| 关 键 词： | N—甲基—2—吡咯腈 合成 |
| 文章编号： | 1003-3467(2003)11-0010-02 |
| 修稿时间： | 2003-07-22 |
Synthesis and Characterization of N-Methyl-2-pyrrolecarbonitrile |
| |
| LIANG Zhi-hong ,ZHAO Lin ,XIE Ya-xiong ,ZHU Yan ,YUAN Si-guo. Synthesis and Characterization of N-Methyl-2-pyrrolecarbonitrile[J]. Henan Chemical Industry, 2003, 0(11): 10-11 |
| |
| Authors: | LIANG Zhi-hong ZHAO Lin XIE Ya-xiong ZHU Yan YUAN Si-guo |
| |
| Affiliation: | LIANG Zhi-hong 1,ZHAO Lin 1,XIE Ya-xiong 2,ZHU Yan 2,YUAN Si-guo 1 |
| |
| Abstract: | N-Methyl-2-pyrrolecarbonitrile(MPC) is synthesized by oximation and dehydration with dichloroethane and corresponding pyrrolealdehyde as raw materials and extractants. The purity of MPC is determined by GC and the structure is characterized by IR and MS. The experimental results show that,the use of dichloroethane as a substituted extractant of ethyl ether has the advantages of safe operation, less solvent loss and lower production cost. |
| |
| Keywords: | N-methyl-2-pyrrolecarbonitrile synthesis |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
