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析出相对Mg-Gd-Y-Nd-Zr合金室温压缩行为的影响
引用本文:唐昌平,李国栋,刘文辉,陈宇强,刘筱,李方伟. 析出相对Mg-Gd-Y-Nd-Zr合金室温压缩行为的影响[J]. 材料导报, 2017, 31(16): 103-106. DOI: 10.11896/j.issn.1005-023X.2017.016.021
作者姓名:唐昌平  李国栋  刘文辉  陈宇强  刘筱  李方伟
作者单位:1. 湖南科技大学材料科学与工程学院,湘潭 411201;高温耐磨材料及制备技术湖南省国防科技重点实验室,湘潭 411201;2. 苏州热工研究院有限公司设备管理部,深圳,518124
基金项目:湖南省自然科学基金(2016JJ5042)
摘    要:采用金相观察、硬度测试、扫描电镜观察、透射电镜观察及室温压缩等手段,研究了时效析出相对Mg-5.5Gd-3.0Y-1.0Nd-1.0Zr合金挤压棒材室温压缩性能的影响。结果表明:该合金具有优异的抗压性能,经225℃/12h时效处理后,合金的抗压强度可达490 MPa,屈服强度可达325 MPa,总压缩应变为8.9%,优异的抗压强度主要归因于合金中与基体呈半共格关系的析出相β′;随着时效程度的进一步增加,合金进入过时效状态,在300℃下时效8h后,合金中析出尺寸达微米级的平衡相β,并在晶界处形成宽度约2 μm的无沉淀析出带,使合金的强化效果减弱;断口分析表明,不同时效状态合金均以解理断裂为主,并在解理面之间以少量韧窝进行连接。

关 键 词:Mg-Gd-Y-Nd-Zr合金  时效  析出相  室温压缩  断口分析

Effects of Precipitates on Compression Behavior of Mg-Gd-Y-Nd-Zr Alloy at Ambient Temperature
TANG Changping,LI Guodong,LIU Wenhui,CHEN Yuqiang,LIU Xiao and LI Fangwei. Effects of Precipitates on Compression Behavior of Mg-Gd-Y-Nd-Zr Alloy at Ambient Temperature[J]. Materials Review, 2017, 31(16): 103-106. DOI: 10.11896/j.issn.1005-023X.2017.016.021
Authors:TANG Changping  LI Guodong  LIU Wenhui  CHEN Yuqiang  LIU Xiao  LI Fangwei
Affiliation:School of Materials Science and Engineering, Hunan University of Science and Technology, Xiangtan 411201;High Temperature Wear Resistant Materials and Preparation Technology of Hunan Province National Defence Science and Technology Laboratory, Xiangtan 411201,Equipment Management Department, Suzhou Nuclear Power Research Institute Company Limited, Shenzhen 518124,School of Materials Science and Engineering, Hunan University of Science and Technology, Xiangtan 411201;High Temperature Wear Resistant Materials and Preparation Technology of Hunan Province National Defence Science and Technology Laboratory, Xiangtan 411201,School of Materials Science and Engineering, Hunan University of Science and Technology, Xiangtan 411201;High Temperature Wear Resistant Materials and Preparation Technology of Hunan Province National Defence Science and Technology Laboratory, Xiangtan 411201,School of Materials Science and Engineering, Hunan University of Science and Technology, Xiangtan 411201;High Temperature Wear Resistant Materials and Preparation Technology of Hunan Province National Defence Science and Technology Laboratory, Xiangtan 411201 and School of Materials Science and Engineering, Hunan University of Science and Technology, Xiangtan 411201;High Temperature Wear Resistant Materials and Preparation Technology of Hunan Province National Defence Science and Technology Laboratory, Xiangtan 411201
Abstract:Effects of precipitates on compression behavior of Mg-5.5Gd-3.0Y-1.0Nd-1.0Zr at ambient temperature were investigated by optical microscopy(OM),hardness testing,scanning electron microscopy(SEM),transmission electron microscopy(TEM)and ambient temperature compression test.The results indicated that the compression property of the alloy was very excellent.After 225 ℃/12 h treated,the compressive strength of the alloy could achieve 490 MPa,the yield strength could achieve 325 MPa,and the total compressive strain could reach 8.9%.The excellent compressive strength was attributed to the β′ precipitate,which was semi-coherent with the magnesium matrix.The alloy became overage as the aging time prolonged.The micrometer scaled equilibrium β phase precipitated from the matrix after aged at 300 ℃ for 8 h.The precipitate free zone with width of about 2 μm was formed at the grain boundary,which weakened the strengthening effect.The fracture analysis indicated that cleavage fracture was the main fracture mode,and the cleavage planes were connected by a small amount of dimples.
Keywords:Mg-Gd-Y-Nd-Zr alloy   aging   precipitate   ambient temperature compression   fracture analysis
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