Ti-48Al粉末压坯烧结过程的内耗行为研究

利用内耗测量技术研究了Ti/Al二元复合粉末压坯的烧结行为。升温测量过程中发现了两个典型的内耗峰,然而这两个内耗峰在随后的降温测量过程都消失了。实验结果表明,低温内耗峰的内耗机制为Al/Al颗粒之间烧结颈的形成,即再结晶过程;高温内耗峰产生于Ti/Al颗粒之间的固相扩散反应(Kirkendall效应)和Ti/Ti颗粒之间的再结晶过程,是一种综合机制。

Study on the Internal Friction Behavior of Ti-48Al Green Compact During Sintering Process

Ti-Al binary powder sintering behavior is studied by internal friction measurements. It is found that two obvious IF peaks were observed in the IF curves during heating while both the two IF peaks vanished in the subsequent cooling in Ti-48Al green compact. The results show that the low temperature IF peak (PL) originates from the transformation from mechanical bonding to metallurgical bonding between Al powder particles, which we named recrystallization. The high temperature IF peak (PH) is the result of two factor comprehensive action of solid phase diffusion at the Ti/Al interface (the process is also named Kirdendall effect) and recrystallization between Ti powder particles.