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Large-scale preparation of hollow graphitic carbon nanospheres
Authors:Jun Feng  Fu Li  Yu-Jun Bai  Fu-Dong Han  Yong-Xin Qi  Ning Lun  Xi-Feng Lu
Affiliation:1. Key Laboratory for Liquid-Solid Structural Evolution and Processing of Materials, Ministry of Education, Shandong University, Jinan 250061, PR China;2. State Key laboratory of Crystal Materials, Shandong University, Jinan 250100, PR China;3. Lunan Institute of Coal Chemical Engineering, Jining 272000, PR China
Abstract:Hollow graphitic carbon nanospheres (HGCNSs) were synthesized on large scale by a simple reaction between glucose and Mg at 550 °C in an autoclave. Characterization by X-ray diffraction, Raman spectroscopy and transmission electron microscopy demonstrates the formation of HGCNSs with an average diameter of 10 nm or so and a wall thickness of a few graphenes. The HGCNSs exhibit a reversible capacity of 391 mAh g−1 after 60 cycles when used as anode materials for Li-ion batteries.
Keywords:Nanostructures   Chemical synthesis   Electron diffraction   Electrochemical properties
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