| 咪唑型离子液体的制备与工艺优化 |
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| 引用本文： | 吉惠杰,杨英杰,郭方超. 咪唑型离子液体的制备与工艺优化[J]. 吉林化工学院学报, 2014, 31(11): 16-18 |
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| 作者姓名： | 吉惠杰 杨英杰 郭方超 |
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| 作者单位： | 吉林化工学院化学与制药工程学院,吉林吉林,132022 |
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| 摘 要： | 主要介绍了由甲基咪唑为初始原料合成1-甲基-3-丁基氟硼酸盐离子液体的合成方法,并对其合成工艺条件进行了优化.实验表明,1-甲基-3-丁基氟硼酸盐离子液体合成适宜条件为:反应溶剂为环己烷,溶剂量100%,物料摩尔比为1 1.1,在回流状态下反应7 h.
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| 关 键 词： | 甲基咪唑 离子液体 合成 优化 |
Synthesis and Process Optimization of [bmim] BF4 Ionic Liquid |
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| JI Hui-jie , YANG Ying-jie , GUO Fang-chao. Synthesis and Process Optimization of [bmim] BF4 Ionic Liquid[J]. Journal of Jilin Institute of Chemical Technology, 2014, 31(11): 16-18 |
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| Authors: | JI Hui-jie YANG Ying-jie GUO Fang-chao |
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| Affiliation: | JI Hui-jie;YANG Ying-jie;GUO Fang-chao;College of Chemical and Pharmaceutical Engineering,Jilin Institute of Chemical Technology; |
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| Abstract: | In this article ,the synthetic method of [ bmim] BF4 ionic liquid by 1-methylimidazole as the initial material is introduced, and the synthesis conditions were optimized. The results showed that the suitable conditions for the synthesis of [ bmim ] BF4 ionic liquid amount was 100% ,the material molar ratio was 1 ： 1.1 was ：the reaction solvent was cyclohexane, the solvent , the reaction time was 7 h under reflux. |
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| Keywords: | 1 -methylimidazole ionic liquid synthesis optimization |
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