| 乙霉威的原位薄层荧光色谱分析方法研究 |
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| 引用本文： | 曾水云,田德美,张世琏. 乙霉威的原位薄层荧光色谱分析方法研究[J]. 精细化工中间体, 2000, 0(5) |
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| 作者姓名： | 曾水云 田德美 张世琏 |
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| 作者单位： | 华中农业大学!湖北武汉430070(曾水云)，华中师范大学农药化学研究所!湖北武汉430079(田德美，张世琏) |
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| 摘 要： | 介绍了用DNS -Cl作为荧光衍生试剂 ,研究了乙霉威的原位薄层荧光色谱扫描微量分析方法。该方法操作简便、灵敏度高、选择性好、专属性强。样品在 1 0～ 50 0ng/点之间有良好的线性关系 ,最低检出限量为 0 .5ng/点。回收率为 94 .52 %～ 1 0 1 .39%。
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| 关 键 词： | 乙霉威 荧光衍生 薄层荧光扫描 |
Quantitative Analysis of Isopropyl 3,4 diethoxyphenyl carbamate by TLC and Fluorimetry Scan Method |
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| ZENG Shui yun ,TIAN De mei ,ZHANG Shi lian. Quantitative Analysis of Isopropyl 3,4 diethoxyphenyl carbamate by TLC and Fluorimetry Scan Method[J]. Fine Chemical Intermediates, 2000, 0(5) |
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| Authors: | ZENG Shui yun TIAN De mei ZHANG Shi lian |
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| Affiliation: | ZENG Shui yun 1,TIAN De mei 2,ZHANG Shi lian 2 |
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| Abstract: | A simple, fast and sensitive method was reported for the quantitative analysis of N phenylcarbamate pesticide with in situ thin layer chromatograph (TLC). There was a linear relation in 10～500ng/spot and as low as 0.5ng/spot of pesticide can be detected. |
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| Keywords: | isopropyl 3 4 diethoxyphenyl carbamate fluorogenic labeling TLC and fluorimetry |
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