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PMN-PT弛豫铁电粉体的溶胶-凝胶法制备及其性质
引用本文:王歆,庄志强,齐雪君. PMN-PT弛豫铁电粉体的溶胶-凝胶法制备及其性质[J]. 无机材料学报, 2002, 17(2): 306-310
作者姓名:王歆  庄志强  齐雪君
作者单位:1. 华南理工大学材料学院, 广州 510640; 2. 中国科学院上海硅酸盐研究所, 上海 200050
基金项目:广东省自然科学基金(990616)
摘    要:以无机盐或氧化物Nb、MgO、TiCl和Pb(AC)、3HO为原材料,柠檬酸和EDTA为复合螫合剂,乙二醇为溶剂,分别制备Nb、Mg-Nb、Ti和Pb的有机化合物前驱液,采用溶胶-凝胶工艺制备PMN-PT弛豫铁电陶瓷粉体及其烧结体.讨论了制备工艺和螯合剂等对金属有机化合物溶液的性质、材料物相形成和介电性能的影响.

关 键 词:溶胶-凝胶法  PMN-PT弛豫铁电体  柠檬酸-EDTA复合螯合剂  无机盐  
文章编号:1000-324X(2002)01-0306-05
收稿时间:2001-03-02
修稿时间:2001-03-02

Preparation and Characterization of PMN-PT Relax Ferroelectric Powders by Sol-Gel Method
WANG Xin,ZHUANG Zhi-Qiang,QI Xue-Jun. Preparation and Characterization of PMN-PT Relax Ferroelectric Powders by Sol-Gel Method[J]. Journal of Inorganic Materials, 2002, 17(2): 306-310
Authors:WANG Xin  ZHUANG Zhi-Qiang  QI Xue-Jun
Affiliation:1. College of Materials Sci. & Eng.; South China University of Technology; Guangzhou 510640; China; 2. Shanghai Institute of Ceramics; Academy of Sciences of China; Shanghai 200050; China
Abstract:PMN-PT relax ferroelectric fine powders were prepared by a sol-gel routes with inorganic compounds, Nb2O5, TiCl4 and Pb(Ac)2·3H2O as raw materials, citric acid and EDTA as co-chelate and ethylene glycol as solvent. The effects of processing technology and complex/ chelate on the properties of organic compounds precursors, the powders synthesis, the phases formation and dielectric properties were discussed.
Keywords:sol-gel method  PMN-PT relax ferroelectric  CA-EDTA co-chelate  inorganic salts
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